HRID262052

反应详情

EQUATION

反应方程式

HRID 262052 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In dry tetrahydrofuran, stoichiometric quantities of isopropyl isocyanate, 5,6,7,8-tetrahydro-4H-cyclohepta[b]thiophen-4-amine hydrochloride, and triethylamine are stirred at room temperature for 2 hours and then heated at reflux for half an hour. The title product is then collected and washed with water.

WORKUP

后处理

  1. temperatureheated
  2. temperatureat reflux for half an hour
  3. customThe title product is then collected
  4. washwashed with water