HRID328560

反应详情

EQUATION

反应方程式

HRID 328560 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
75 °C

PROCEDURE

实验过程

Magnesium glycinate was prepared by reacting 5 grams of glycine with 3.1 grams of basic magnesium carbonate (26.3% Mg) in 15 grams of water. The mixture was heated at 75° C. for 1/2 hour with agitation. The hot solution was then added to 113 grams of zirconyl nitrate (7.9% Zr) with stirring. After the addition of 1.5 grams of aluminum hydroxide powder (28.8% Al), the mixture was reacted with agitation at 75° C. for 1/2 hour. To the resultant clear solution was added 7.9 grams of 2/3 basic aluminum sulfate, Al(OH)2SO4 (3.1% Al). The solution was then oven dried at 58° C. under a vacuum of 328 mm of Hg. The product contained 1.2% Mg, 13.2% glycine, 1.5% Al, 24.3% Zr, 4.02% SO4 and 29.5% nitrate.

WORKUP

后处理

  1. customthe mixture was reacted with agitation at 75° C. for 1/2 hour
  2. customoven dried at 58° C. under a vacuum of 328 mm of Hg