HRID403986
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The compound of example 393 (75 mg, 0.150 mmol) was taken in THF (3 mL) and MeOH (1 mL) and to this reaction mixture, 1 N LiOH (31.47 mg, 0.75 mmol) was added and stirred at room temperature for 2-3 h. After completion of the reaction, solvent was evaporated and the residue obtained was dissolved in water and acidified with 1 N HCl to obtain the title compound, which was filtered and dried.
WORKUP
后处理
- customAfter completion of the reaction, solvent
- customwas evaporated
- customthe residue obtained