huagongshe.com
HRID411000

反应详情

EQUATION

反应方程式

HRID 411000 的结构方程式

REACTANTS

反应物

2
结构：CN
HCID6329

Methylamine

CH5N

结构：CCOC(=O)c1ccc([N+](=O)[O-])c(F)c1
HCID45036938

Ethyl 3-fluoro-4-nitrobenzoate

C9H8FNO4

PRODUCTS

生成物

1
结构：CCOC(=O)c1ccc([N+](=O)[O-])c(NC)c1
HCID67333336

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

3-Methylamino-4-nitro-benzoic acid ethyl ester (2.8 g) was prepared by following General Procedure A starting from 3-fluoro-4-nitro-benzoic acid ethyl ester (3 g) and 2 M methylamine in THF (15 mL) in DMF (15 mL).