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A method in which a solution of polymetaphenyleneisophthalamide is prepared by subjecting metaphenylenediamine and isophthalic acid chloride to a low-temperature solution polymerization procedure in N,N-dimethylacetamide; hydrochloric acid contained, as a by-product, in the resultant polymer solution is neutralized with calcium hydroxide; the polymer solution containing the produced calcium chloride is subjected to a dry-spinning procedure to produce polymetaphenylenediamine isophthalamide filaments. (Japanese Examined Patent Publication No. 35-14,399, U.S. Pat. No. 3,360,595)
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- customA method in which a solution of polymetaphenyleneisophthalamide is prepared