HRID5159

反应详情

EQUATION

反应方程式

HRID 5159 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Using the procedure of Step A of Example 8, 27.2 g of 7-amino-cephalosporanic acid, 170 ml of the etherate of of boron trifluoride, 131 ml of propanol and 128 ml of triethylamine were reacted to obtain 17.4 g of raw product which was purified with hot hydrochloric acid and ammonium hydroxide to obtain 7.45 g of 3-propoxymethyl-7-amino-ceph-3-eme-4-carboxylic acid.

WORKUP

后处理

  1. customwere reacted
  2. customto obtain 17.4 g of raw product which
  3. customwas purified with hot hydrochloric acid and ammonium hydroxide