HRID6585

反应详情

EQUATION

反应方程式

HRID 6585 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

35 mmol of benzyl bromide (BzBn, 35 mmol of ethyl 4-hydroxybenzoate (10), 14 g of Cs2CO3 and 40 ml of DMF were combined and stirred at RT ove night. Then the reaction mixture was poured into water and the product was collected by extraction. The organic solution was washed with brine and dried over MgSO4. After evaporation of solvent, pure product was obtained in yield of 100%.

WORKUP

后处理

  1. customthe product was collected by extraction
  2. washThe organic solution was washed with brine
  3. dry with materialdried over MgSO4
  4. customAfter evaporation of solvent
  5. custompure product was obtained in yield of 100%