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HRID866043

反应详情

EQUATION

反应方程式

HRID 866043 的结构方程式

REACTANTS

反应物

6
结构：Nc1c([N+](=O)[O-])cc([N+](=O)[O-])cc1[N+](=O)[O-]
HCID10271

2,4,6-Trinitroaniline

C6H4N4O6

结构：CC(=O)N(C)C
HCID31374

Dimethylacetamide

C4H9NO

结构：CC[O-].[Na+]
HCID2723922

Ethanol, sodium salt

C2H5NaO

结构：CC(C)[O-].[Na+]
HCID10920443

2-Propanol, sodium salt (1:1)

C3H7NaO

结构：C[O-].[Na+]
HCID10942334

Methanol, sodium salt

CH3NaO

结构：CC(C)(C)[O-].[Na+]
HCID23676156

Sodium t-butoxide

C4H9NaO

PRODUCTS

生成物

1
结构：Nc1c([N+](=O)[O-])cc([N+](=O)[O-])c(N)c1[N+](=O)[O-]
HCID15396

1,3-Benzenediamine, 2,4,6-trinitro-

C6H5N5O6

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Similarly, when Example 4(a) is repeated except that DMSO is replaced by a volumetrically equivalent amount of DMF or DMAC and sodium methoxide is replaced by a stoichiometrically equivalent amount of sodium ethoxide, sodium n-propoxide, sodium isopropoxide, or sodium tert-butoxide respectively, a mixture of picramide and DATB is produced. The DATB is purified by crystallization from DMF and DMSO.