Ammonium → 4-Methoxy-3,5-dimethylbenzaldehyde

HRID 937655Notes

Reaction equation

HRID 937655 reaction equation
[Br:1][c:2]1[cH:3][c:4]([CH3:11])[c:5]([O:9][CH3:10])[c:6]([CH3:8])[cH:7]1.[CH2:12]([Li:13])[CH2:14][CH2:15][CH3:16].[CH2:24]1[O:25][CH2:26][CH2:27][CH2:28]1.[CH3:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34].[CH3:35][CH2:36][O:37][C:38](=[O:39])[CH3:40].[Cl-:22].[NH4+:23].[O:17]=[CH:18][N:19]([CH3:20])[CH3:21]>>[c:2]1([CH:18]=[O:17])[cH:3][c:4]([CH3:11])[c:5]([O:9][CH3:10])[c:6]([CH3:8])[cH:7]1

Participants

9

Reactant 8

HCID 223AmmoniumHCID 312ChlorideHCID 6228DimethylformamideHCID 8028TetrahydrofuranHCID 8058HexaneHCID 8857Ethyl AcetateHCID 2786544-Bromo-2,6-dimethylanisoleHCID 178418339Butyllithium

Product 1

HCID 27585734-Methoxy-3,5-dimethylbenzaldehyde

Sources & evidence

ORD record
ord-44430fc78a824eac8c4d890656e207e2
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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