Chloride → 2,2,6,7-Tetramethyl-1-benzofuran-3(2H)-one

HRID 955701Notes

Reaction equation

HRID 955701 reaction equation
[Al+3:28].[C:1]([Cl:2])(=[O:3])[C:4]([Cl:5])=[O:6].[CH2:31]1[O:32][CH2:33][CH2:34][CH2:35]1.[CH3:12][c:13]1[c:14]([O:15][C:16]([C:17](=[O:18])[OH:19])([CH3:20])[CH3:21])[cH:22][cH:23][cH:24][c:25]1[CH3:26].[Cl-:27].[Cl-:29].[Cl-:30].[O:7]=[CH:8][N:9]([CH3:10])[CH3:11]>>[CH3:12][c:13]1[c:14]2[c:22]([cH:23][cH:24][c:25]1[CH3:26])[C:17](=[O:19])[C:16]([CH3:20])([CH3:21])[O:15]2

Participants

7

Reactant 6

HCID 312Chloride3×HCID 6228DimethylformamideHCID 8028TetrahydrofuranHCID 65578Oxalyl chlorideHCID 104727Aluminum CationHCID 15320132-(2,3-Dimethylphenoxy)-2-methylpropanoic acid

Product 1

HCID 231142662,2,6,7-Tetramethyl-1-benzofuran-3(2H)-one

Sources & evidence

ORD record
ord-1f7fc6cdc6cb447ea680c5f227e9dd1a
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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