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Dichloromethane → 1-(4-Dimethylamino-piperidin-1-yl)-2-hydroxy-2,2-di-thiophen-2-ylethanone

HRID 220332
Notes
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Reaction equation

HRID 220332 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](=[O:10])[C:7](O)=[O:8].C(Cl)Cl.C(Cl)(=O)C(Cl)=O.[CH3:20][N:21]([CH3:28])[CH:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1.CCN(C(C)C)C(C)C.C1COCC1.[S:43]1[CH:47]=[CH:46][CH:45]=[C:44]1[Mg]Br>CN(C1C=CN=CC=1)C.CN(C=O)C>[CH3:20][N:21]([CH3:28])[CH:22]1[CH2:27][CH2:26][N:25]([C:7](=[O:8])[C:6]([OH:10])([C:2]2[S:1][CH:5]=[CH:4][CH:3]=2)[C:44]2[S:43][CH:47]=[CH:46][CH:45]=2)[CH2:24][CH2:23]1
ParticipantsConditionsProcedureWorkupSources & evidenceReaction notes

Participants

10

Reactant 7

HCID 6344DichloromethaneHCID 8028Tetrahydrofuran2×HCID 65578Oxalyl chlorideHCID 776942-Thiopheneglyoxylic acidHCID 81531DiisopropylethylamineHCID 417391N,N-Dimethylpiperidin-4-amineHCID 178418438HCID 178418438, compound

Product 1

HCID 598285271-(4-Dimethylamino-piperidin-1-yl)-2-hydroxy-2,2-di-thiophen-2-ylethanone

Reagents, catalysts & solvents 2

HCID 142844-(Dimethylamino)pyridineCatalystHCID 6228DimethylformamideSolvent

Conditions

Temperature
0 °C

Procedure

To a stirred solution of 2-thiopheneglyoxylic acid (1.0 g, 6.4 mmol) in DCM (100 mL, 2 mol), was added oxalyl chloride (596 μL, 7 mmol) and a catalytic amount of DMF. The mixture was stirred for 2 hours and then was cooled at 0° C. in an ice bath. Dimethyl-piperidin-4-ylamine (821 mg, 6.4 mmol), DIPEA (1.7 mL, 9.6 mmol) and DMAP (20 mg, 0.1 mmol) were added, and the mixture was stirred for 2 hours. The solvent was removed under reduced pressure and the crude mixture was then dissolved in DCM (60 mL), washed with a saturated bicarbonate solution (50 mL), and dried over MgSO4. The solvent was removed under reduced pressure and the crude material was then dissolved in THF (50 mL, 0.6 mol) and cooled to 0° C. in an ice bath. To the stirred solution was added 1.0 M thiophen-2-yl magnesium bromide in THF (7.7 mL, 7.7 mmol) was added. The mixture was stirred for 30 minutes, then quenched with a saturated bicarbonate solution (50 mL) and DCM (50 mL). The organic was taken and dried over MgSO4, and the solvent was removed under reduced pressure, to afford the title compound (1.5 g).

Workup

  1. stirringthe mixture was stirred for 2 hours
  2. customThe solvent was removed under reduced pressure
  3. dissolutionthe crude mixture was then dissolved in DCM (60 mL)
  4. washwashed with a saturated bicarbonate solution (50 mL)
  5. dry with materialdried over MgSO4
  6. customThe solvent was removed under reduced pressure
  7. temperaturecooled to 0° C. in an ice bath
  8. additionwas added
  9. stirringThe mixture was stirred for 30 minutes
  10. customquenched with a saturated bicarbonate solution (50 mL) and DCM (50 mL)
  11. dry with materialdried over MgSO4
  12. customthe solvent was removed under reduced pressure

Sources & evidence

ORD record
ord-61b81f85042e4cc6a30b78aa8ac3033d
Source dataset
uspto-grants-2012_06
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US08202891B2

Reaction notes

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On this pageParticipantsConditionsProcedureWorkupSources & evidenceReaction notes