Azobisisobutyronitrile → Allyl methacrylate

HRID 364156

反応式

HRID 364156 の反応式
C(N1CCCC1=O)=C.[C:9]([O:14][CH2:15][CH2:16][CH2:17]CCCCCCCCC)(=[O:13])[C:10]([CH3:12])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>O>[C:9]([O:14][CH2:15][CH:16]=[CH2:17])(=[O:13])[C:10]([CH3:12])=[CH2:11]

参加物

6

反応物 4

HCID 6547AzobisisobutyronitrileHCID 6917N-vinyl-2-pyrrolidoneHCID 8906Lauryl MethacrylateHCID 178435178HCID 178435178、化合物

生成物 1

HCID 7274Allyl methacrylate

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (based on to the entire mixture) to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% dodecyl methacrylate. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 76 wt.-% water at G=0.048 MPa. The soluble extractable portion was 2%.

後処理

  1. additionwas added in the amount of 3 wt.-% (

出典と根拠

ORDレコード
ord-0c898061a2e84a4b86bc75b954ef6864
出典データセット
uspto-grants-1986_08
特許番号
US04604440

関連ノート

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