Acetone → Anisole

HRID 1257966Notes

Reaction equation

HRID 1257966 reaction equation
[CH3:1][C:2]([CH3:4])=[O:3].[CH2:5]([C:7](C)=O)[CH3:6].C([C:14](C)=[O:15])C(C)C.[C:17]1(C)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(O)CO.CS(C)=O.CC(N(C)C)=O.CN(C)C=O.O1CCCC1.CCCCCCC.C(OCC)(=O)C>[C:2]1(=[O:3])[CH2:4][CH2:7][CH2:5][CH2:6][CH2:1]1.[C:17]1([O:15][CH3:14])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

13

Reactant 4

HCID 180AcetoneHCID 1140TolueneHCID 6569Methyl Ethyl KetoneHCID 7909Methyl Isobutyl Ketone

Product 2

HCID 7519AnisoleHCID 7967Cyclohexanone

Reagents, catalysts & solvents 7

HCID 174Ethylene GlycolSolventHCID 679Dimethyl SulfoxideSolventHCID 6228DimethylformamideSolventHCID 8028TetrahydrofuranSolventHCID 8857Ethyl AcetateSolventHCID 8900HeptaneSolventHCID 31374DimethylacetamideSolvent

Procedure

About the insulating resin sheet 5, a resin varnish is prepared by dissolving, mixing and stirring the resin composition for forming the insulating resin layer 51 in an organic solvent such as acetone, methyl ethyl ketone, methyl isobutyl ketone, toluene, ethyl acetate, cyclohexanone, heptane, cyclohexanecyclohexanone, tetrahydrofuran, dimethylformamide, dimethylacetamide, dimethyl sulfoxide, ethylene glycol, cellosolves, carbitols and anisole, using any of various mixers such as an ultrasonic dispersion type, a high-pressure impact dispersion type, a high-speed rotating dispersion type, a bead mill type, a high speed shearing dispersion type and a rotation/revolution type mixers.

Workup

  1. customAbout the insulating resin sheet 5, a resin varnish is prepared
  2. dissolutionby dissolving
  3. additionmixing

Sources & evidence

ORD record
ord-672f48beb640456eb9f94a47f7ec3e79
Source dataset
uspto-grants-2013_06
Patent number
US08465837B2

Reaction notes

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