huagongshe.com
HRID1817282

反应详情

EQUATION

反应方程式

HRID 1817282 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)c1ccc(Br)cc1
HCID7466

Ethanone, 1-(4-bromophenyl)-

C8H7BrO

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CN1CCNCC1
HCID53167

1-Methylpiperazine

C5H12N2

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(N2CCN(C)CC2)cc1
HCID33551

Acetophenone, 4'-(4-methyl-1-piperazinyl)-

C13H18N2O

收率 82%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cu]
催化剂HCID23978

Copper

Cu

结构：[I][Cu][I]
催化剂HCID83717

Copper iodide (CuI2)

CuI2

PROCEDURE

实验过程

In a procedure identical to Example 53, 4-bromoacetophenone was reacted with N-methylpiperazine in the presence of potassium carbonate, copper and copper iodide to furnish the desired product in 82% yield.