反应详情

3-Chloro-5,6-dimethoxy-benzo[b]thiophene-2-carbonyl chloride (2.0 g) and 2,6-dimethylmorpholine (1.82 g) was suspended in tetrahydrofuran (15 ml) and triethylamine (0.96 ml) was added and stirring continued at room temperature for weekend. Water was added, pH adjusted to 3 by HCl, and the precipitate filtered.

1. waitcontinued at room temperature for weekend
2. filtrationthe precipitate filtered