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HRID270674

反应详情

EQUATION

反应方程式

HRID 270674 的结构方程式

REACTANTS

反应物

7
结构：C=O
HCID712

Formaldehyde

CH2O

结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：BrB(Br)Br
HCID25134

Boron tribromide

BBr3

结构：O=C(OO)c1cccc(Cl)c1
HCID70297

Benzenecarboperoxoic acid, 3-chloro-

C7H5ClO3

结构：CN1CCCN(C)C1=O
HCID81646

2(1H)-Pyrimidinone, tetrahydro-1,3-dimethyl-

C6H12N2O

结构：CC(C)(C)CS(N)(=O)=O
HCID18348400

未命名化合物

结构：CO[K]
HCID178502595

未命名化合物

PRODUCTS

生成物

1
结构：c1ccc2c3c(ncc2c1)COCO3
HCID70329483

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

3
结构：ClCCCl
溶剂HCID11

1,2-Dichloroethane

C2H4Cl2

结构：O=S(=O)(O)O
溶剂HCID1118

Sulfuric acid

H2O4S

结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

Reaction Conditions: (1) MeOK in DMPU; (2) MCPBA in CH2Cl2; (3) POCl3 in DCE; (4) BBr3 in CH2Cl2; (5) HCHO solution in 40% H2SO4 by procedure of Synthesis of 1,3-oxazino[5,6-c]isoquinolines and related compounds. Miyoko Toyama and Hirotaka Otomasu, Chem. Pharm. Bull. 33(12), 5543-5546, 1985; (6) Fluororination procedure by Uchibori, Y.; Umeno, M.; Yoshiokai, H.; Heterocycles, 1992, 34 (8), 1507-1510

WORKUP

后处理

  1. customReaction Conditions