Chloride → N-Boc-3-mesyloxypiperidine

HRID 829114Notes

Reaction equation

HRID 829114 reaction equation
[C:1](=[O:2])([O:3][C:4]([CH3:5])([CH3:6])[CH3:7])[N:8]1[CH2:9][CH:10]([OH:14])[CH2:11][CH2:12][CH2:13]1.[C:28](=[O:29])([OH:30])[O-:31].[CH3:15][CH2:16][N:17]([CH2:18][CH3:19])[CH2:20][CH3:21].[CH3:23][S:24](=[O:25])(=[O:26])[OH:27].[CH3:38][CH2:39][O:40][C:41](=[O:42])[CH3:43].[Cl-:22].[Na+:32].[O:33]1[CH2:34][CH2:35][CH2:36][CH2:37]1>>[C:1](=[O:2])([O:3][C:4]([CH3:5])([CH3:6])[CH3:7])[N:8]1[CH2:9][CH:10]([O:14][S:24]([CH3:23])(=[O:25])=[O:26])[CH2:11][CH2:12][CH2:13]1

Participants

9

Reactant 8

HCID 312ChlorideHCID 769Bicarbonate IonHCID 923Sodium ionHCID 6395Methanesulfonic AcidHCID 8028TetrahydrofuranHCID 8471TriethylamineHCID 8857Ethyl AcetateHCID 5456991-Boc-3-hydroxypiperidine

Product 1

HCID 568122N-Boc-3-mesyloxypiperidine

Sources & evidence

ORD record
ord-fdbc19b13dde47c6b0d38604a4ce6e20
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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