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HRID986381

反应详情

EQUATION

反应方程式

HRID 986381 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：CC(C)(C)OC(=O)N[C@@H](Cc1ccccc1)C(N)=O
HCID7020416

Boc-L-phenylalaninamide

C14H20N2O3

PRODUCTS

生成物

2
结构：CN1CCOCC1
HCID7972

4-Methylmorpholine

C5H11NO

结构：Cl.NC(=O)[C@@H](N)Cc1ccccc1
HCID11953719

L-Phenylalaninamide hydrochloride

C9H13ClN2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Two minutes later, a solution of PheNH2HCl (1.2 g, 0.6 mmol), obtained by cleavage of the t-butoxycarbonyl group from BocPheNH2 with 4.5N HCl in EtOAc, and NMM (0.6 g, 6 mmoles) in DMF is added thereto.