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Formate → (R)-propyl 2-(7-amino-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate

HRID 476227
Notes
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Reaction equation

HRID 476227 reaction equation
P([O-])([O-])([O-])=O.[Na+].[Na+].[Na+].[CH:9]([O-:11])=[O:10].[Na+].[NH2:13][C@@H:14]([C:16](O)=O)[CH3:15].C1N=C(N)C2N=CN([C@@H]3O[C@H](COP(OP(OC[C@H]4O[C@@H:47]([N:49]5[CH:54]=[C:53]([C:55](N)=O)[CH2:52][CH:51]=[CH:50]5)[C@H:46](O)[C@@H:45]4O)(O)=O)(O)=O)[C@@H](O)[C@H]3O)C=2N=1.[CH3:63][C:64]1[C:69](O)=C(C=O)C(COP(O)(O)=O)=CN=1.[C:79]([O-])(=O)C(C)O.C([O-])=O.Cl>O>[NH2:13][C@H:14]1[CH2:16][N:49]2[C:47]3[C:52]([C:53]([CH2:55][C:9]([O:11][CH2:63][CH2:64][CH3:69])=[O:10])=[C:54]2[CH2:79][CH2:15]1)=[CH:51][CH:50]=[CH:45][CH:46]=3
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

10

Reactant 8

HCID 283FormateHCID 313Hydrochloric AcidHCID 1051Pyridoxal 5'-phosphateHCID 24243Trisodium PhosphateHCID 71080D-AlanineHCID 91435LactateHCID 439153Nadh
HCID 2723810
Sodium Formate

Product 1

HCID 58349691(R)-propyl 2-(7-amino-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetateYield 80%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Sodium phosphate, dibasic (3.8 equiv.) and sodium formate (266 equiv.) were added to a solution of D-alanine (38 equiv.) in water. The pH was measured as 7.6. NAD (0.04 equiv.), Pyridoxal-5-phosphate (0.11 equiv.), Lactate dehydrogenase (LDH) (1 equiv.), Formate dehydrogenase (FDH) (1 equiv.), and Amine-Transaminase ATA117 (1 equiv.) were added under stirring and slowly dissolved. The measured pH was 7.3. The mixture was aged at 22° C. for 1 h. The flask was flushed with nitrogen and propyl (7-oxo-6,7,8,9-tetrahydropyrido[1,2-a]-indol-10-yl)acetate from Step 5 was added as a DMSO (0.06 M) solution. The reaction was adjusted to pH 7.2 and aged at 30° C. overnight under nitrogen atmosphere. Upon completion of the reaction as determined by HPLC, the pH of the reaction was adjusted to pH 4.0 with 6N HCl and Celite (20 g per L) was added. After stirring for 1 hr the reaction was filtered through a Celite bed and the filter cake was washed twice with 0.1N HCl. The combined aqueous filtrate was extracted with 1 volume of MTBE. The organic layer did not contain amine and was discarded. The aqueous layer was diluted with an equal volume of MTBE and the pH of the mixture was adjusted to pH 9.5 using 5N NaOH. The two phases were separated and the aqueous layer was extracted with MTBE. The spent aqueous layer had no detectable amine and was discarded. The combined organic layers were washed with dilute sodium carbonate and dried over Na2SO4. Evaporation of the volatiles afforded the crude title compound (80%). The ee was determined as 99% by SFC assay.

Workup

  1. dissolutionslowly dissolved
  2. customThe flask was flushed with nitrogen and propyl (7-oxo-6,7,8,9-tetrahydropyrido[1,2-a]-indol-10-yl)acetate from Step 5
  3. additionwas added as a DMSO (0.06 M) solution
  4. waitaged at 30° C. overnight under nitrogen atmosphere
  5. customUpon completion of the reaction
  6. additionwas added
  7. stirringAfter stirring for 1 hr the reaction
  8. filtrationwas filtered through a Celite bed
  9. washthe filter cake was washed twice with 0.1N HCl
  10. extractionThe combined aqueous filtrate was extracted with 1 volume of MTBE
  11. additionThe aqueous layer was diluted with an equal volume of MTBE
  12. customThe two phases were separated
  13. extractionthe aqueous layer was extracted with MTBE
  14. washThe combined organic layers were washed with dilute sodium carbonate
  15. dry with materialdried over Na2SO4
  16. customEvaporation of the volatiles

Sources & evidence

ORD record
ord-8723912062624398ba70fdb5dfdb76d6
Source dataset
uspto-grants-2014_01
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US08637671B2

Reaction notes

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